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CAS No. 5137-55-3
Content 75%
Packing 175kg/drum 850kg/IBC
| Name | Aliquat 336 |
| Synonyms | TOMAC Aliquat CAPRIQUAT TricapryL Aliquat 336 Methyltrioctylammonium chloride TRIOCTYLMETHYLAMMONIUM CHLORIDE TRICAPRYLMETHYLAMMONIUM CHLORIDE Methyl trioctyl ammonium chloride Trioctyl Methyl Ammonium Chloride TRI-N-OCTYLMETHYLAMMONIUM CHLORIDE TRICAPRYLYLMETHYLAMMONIUM CHLORIDE TRICAPRYLYL MONOMETHYLAMMONIUM CHLORIDE |
| CAS | 5137-55-3 |
| EINECS | 225-896-2 |
| InChI | InChI=1/C25H53N/c1-4-7-10-13-16-19-22-25(26,23-20-17-14-11-8-5-2)24-21-18-15-12-9-6-3/h4-24,26H2,1-3H3/p+1 |
| InChIKey | XKBGEWXEAPTVCK-UHFFFAOYSA-M |
| Molecular Formula | C25H54ClN |
| Molar Mass | 404.16 |
| Density | 0.884g/mLat 25°C(lit.) |
| Melting Point | -20°C |
| Boling Point | 240°C |
| Flash Point | >230°F |
| Water Solubility | Partially insoluble |
| Vapor Presure | 0Pa at 25℃ |
| Appearance | Viscous Liquid |
| Color | Colourless to pale orange |
| Odor | Ammonical |
| BRN | 4039255 |
| Storage Condition | under inert gas (nitrogen or Argon) at 2-8°C |
| Stability | Stable. Incompatible wth strong oxidizing agents. Hygroscopic. |
| Sensitive | Hygroscopic |
| Refractive Index | n20/D 1.4665(lit.) |
| Risk Codes | R22 – Harmful if swallowed R38 – Irritating to the skin R41 – Risk of serious damage to eyes R50/53 – Very toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment. R36/37/38 – Irritating to eyes, respiratory system and skin. R20/21/22 – Harmful by inhalation, in contact with skin and if swallowed. R34 – Causes burns |
| Safety Description | S26 – In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S39 – Wear eye / face protection. S60 – This material and its container must be disposed of as hazardous waste. S61 – Avoid release to the environment. Refer to special instructions / safety data sheets. S36 – Wear suitable protective clothing. S45 – In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) S36/37/39 – Wear suitable protective clothing, gloves and eye/face protection. |
| UN IDs | UN 2810 6.1/PG 3 |
| WGK Germany | 3 |
| RTECS | UZ2997500 |
| FLUKA BRAND F CODES | 3-10 |
| HS Code | 29239000 |
| Hazard Class | 6.1 |
| Packing Group | III |
| LogP | 4.5 at 25℃ |
| Use | Methyl trioctyl ammonium chloride, also known as trioctyl methyl ammonium chloride, is a halogenated quaternary ammonium salt. Quaternary ammonium salt is a kind of cationic surfactant, among which halogenated quaternary ammonium salt (R1R2R3R4N X-) series compounds are widely used in daily chemical industry, textile, printing and dyeing, mining, asphalt, construction, plastic processing, petroleum exploitation, petrochemical industry and other fields, playing an important role. C8 and C10 chain mixture, C8 occupies the main body. Used as metal extractant and phase transfer catalyst. Phase transfer reagent |
| preparation | weigh 1000g of trioctylamine and place it in a beaker, add concentrated hydrochloric acid (HCl adds a total of about 103g) drop by drop, stir by magnetic force, evaporate with a constant temperature water bath to remove about 80% of the water after the neutralization reaction, and then dry the product trioctylammonium chloride in vacuum. Weights 1000g of trioctylammonium chloride and 235g of dimethyl carbonate respectively, and add them to a 10L reaction kettle in turn, after purging with nitrogen to drive away the air in the kettle, the reaction is carried out in a closed manner. The reaction temperature is 170 ℃, and stirring is started after the reaction temperature reaches 170 ℃. The reaction time is 8 hours. After the reaction is over, about 1026g of methyl trioctylammonium chloride was prepared. |
| production method | 1.396g (1 mol) N235 and 300 ml ethanol are mixed in an autoclave by autoclave method, and the kettle body is used for ice-acetone cooling. Then pour 2 moles of methyl chloride (pre-frozen and liquefied, collected in a conical flask), immediately close the autoclave, stir and heat until 100 react at a pressure of <10kg/cm2 for 4-5 hours, then cool to room temperature and release residual methyl chloride. Then vacuum distillation removes ethanol to obtain brown product, weighing about 430 grams (95-100%). 2. By atmospheric pressure, 100 ml of 52g, 0.2 mol) N235 and isooctanol with a volume ratio of 1.5:1 to N236 are placed in a tubular reactor, and methyl chloride is introduced at a flow rate of 150 ml/min for about 20 minutes. Then heat to 130 ℃. Methyl chloride was introduced at the flow rate of tiny bubbles and reacted for 5-7 hours. Cooling, the reactants are transferred to the liquid film evaporator, and the solvent is evaporated by vacuum distillation at 120-130 ℃/3-5mm to obtain the product. The conversion rate is 60-70%. |
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